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CURRICULUM VITAE

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Name: Joaquim
Surnames: Carrasqueiro Marçalo de Almeida
Born: 26 October 1957; Lisbon, Portugal
Nationality: Portuguese

Phone: +351-21-9946170
E-mail: jmarcalo (add @itn.pt)

Education

  • 1990 - PhD in Chemistry, Instituto Superior Técnico, Lisbon.
  • 1980 - Graduation in Chemical Engineering, Instituto Superior Técnico, Lisbon.

Professional Employment Career

  • Since 2006 – Principal researcher, Instituto Tecnológico e Nuclear.
  • 1991-2005 – Auxiliary researcher, Instituto Tecnológico e Nuclear.
  • 1984-1990 – Research assistant, Instituto de Ciências e Engenharia Nucleares, LNETI/INETI.
  • 1980-1983 – Research student, Instituto de Ciências e Engenharia Nucleares, LNETI/INETI.
  • April 2008-present – Coordinator-Chemical and Radiopharmaceutical Sciences Unit, Instituto Tecnológico e Nuclear.
  • November 2007-present – Coordinator-Inorganic and Organometallic Chemistry Group, Instituto Tecnológico e Nuclear.
  • Member - Research Unit «Glass and Ceramics for the Arts», Universidade Nova de Lisboa.

Membership of Professional Societies

  • 1978-present – Member of the Portuguese Society of Chemistry.

Scientific Specialization

  • Inorganic Chemistry; Physical Chemistry; Radiochemistry; Analytical Chemistry.

Main Scientific Area of Research

  • Lanthanide and actinide chemistry; gas-phase ion chemistry; mass spectrometry; thermochemistry; glass science.

Teaching Activities
  • 2001-present – Radiochemistry and Mass Spectrometry/Instrumental Analysis I; MSc course in Conservation and Restoration, Departamento de Conservação e Restauro/Universidade Nova de Lisboa.
Scientific Works
  • "Modelos Estereoquímicos na Química de Coordenação e Organometálica de Lantanídeos e Actinídeos - Aplicações a Complexos de Tório (IV) com Boratos de Polipirazolilo", PhD Thesis, IST, Lisboa, 1990.
  • Author or co-author of 50 original publications in Refereed Journals; 4 original publications in National Journals; 19 original publications in Proceedings of national and international conferences; 112 communications to national and international conferences.
Selected Publications

  • Molecular Uranates - Laser Synthesis of Uranium Oxide Anions in the Gas Phase, J. Marçalo, M. Santos, A. Pires de Matos, J. K. Gibson, Inorg. Chem., Web: May 8, 2009.
  • Gas-Phase Reactions of Doubly Charged Lanthanide Cations with Alkanes and Alkenes. Trends in Metal(2+) Reactivity, J. Marçalo, M. Santos, A. Pires de Matos, J. K. Gibson, R. G. Haire, J. Phys. Chem. A 2008, 112, 12647-12656.
  • FTICR/MS Studies of Gas-Phase Actinide Ion Reactions: Fundamental Chemical and Physical Properties of Atomic and Molecular Actinide Ions and Neutrals, J. K. Gibson, R. G. Haire, J. Marçalo, M. Santos, J. P. Leal, A. Pires de Matos, R. Tyagi, M. K. Mrozik, R. M. Pitzer, B. E. Bursten, Eur. Phys. J. D 2007, 45, 133-138.
  • Gas-Phase Reactions of Hydrocarbons with An+ and AnO+ (An = Th, Pa, U, Np, Pu, Am, Cm): The Active Role of 5f Electrons in Organoprotactinium Chemistry, J. K. Gibson, R. G. Haire, J. Marçalo, M. Santos, A. Pires de Matos, M. K. Mrozik, R. M. Pitzer, B. E. Bursten, Organometallics 2007, 26, 3947-3956.
  • Identification of 7,4’-Dihydroxy-5-methoxyflavylium in «Dragon’s Blood». To be or not to be an Anthocyanin, M. J. Melo, M. Sousa, A. J. Parola, J. S. Seixas de Melo, F. Catarino, J. Marçalo, F. Pina, Chem. Eur. J. 2007, 13, 1417-1422.
  • Actinide-Transition Metal Heteronuclear Ions and Their Oxides: {IrUO}+ as an Analogue to Uranyl, M. Santos, J. Marçalo, A. Pires de Matos, J. K. Gibson, R. G. Haire, Eur. J. Inorg. Chem. 2006, 3346-3349.
  • New Developments in Gas-Phase Actinide Ion Chemistry, J. K. Gibson, J. Marçalo, Coord. Chem. Rev. 2006, 250, 776-783.
  • The Uranium-Nitrogen Bond in U(IV) Complexes Supported by the Hydrotris(3,5-dimethylpyrazolyl)borate Ligand, M. Silva, M. A. Antunes, M. Dias, A. Domingos, I. Cordeiro dos Santos, J. Marçalo, N. Marques, Dalton Trans. 2005, 3353-3358.
  • Oxidation Studies of Dipositive Actinide Ions, An2+ (An = Th, U, Np, Pu, Am) in the Gas Phase: Synthesis and Characterization of the Isolated Uranyl, Neptunyl, and Plutonyl Ions UO22+(g), NpO22+(g), and PuO22+(g), J. K. Gibson, R. G. Haire, M. Santos, J. Marçalo, A. Pires de Matos, J. Phys. Chem. A 2005, 109, 2768-2781.
  • FTICR-MS Study of the Gas-Phase Thermochemistry of Americium Oxides, M. Santos, J. Marçalo, J. P. Leal, A. Pires de Matos, J. K. Gibson, R. G. Haire, Int. J. Mass Spectrom. 2003, 228, 457-465.
  • Characterization of Glasses by FTICR Mass Spectrometry, M. Santos, J. Marçalo, A. Pires de Matos, Phys. Chem. Glasses 2002, 43C, 421-423.
  • Organolanthanide Chemistry in the Gas Phase, J. Marçalo, A. Pires de Matos, J. Organomet. Chem. 2002, 647, 216-224.
  • Reactivity of Lanthanide, Group 2, and Group 3 Metal and Metal Oxide Cations with Pentamethylcyclopentadiene: Gas Phase Synthesis of Cyclopentadienyl Cations, J. Marçalo, A. Pires de Matos, W. J. Evans, Organometallics 1997, 16, 3845-3850.
  • Gas Phase Actinide Ion Chemistry: Activation of Alkanes and Alkenes by Thorium Cations, J. Marçalo, J. P. Leal, A. Pires de Matos, Int. J. Mass Spectrom. Ion Processes 1996, 157/158, 265-274.
  • The Bare Uranyl (2+) Ion, UO22+, H. H. Cornehl, C. Heinemann, J. Marçalo, A. Pires de Matos, H. Schwarz, Angew. Chem. Int. Ed. Engl. 1996, 35, 891-894.
  • Gas Phase Synthesis and FT/ICR Mass Spectrometric Characterization of Sandwich Complexes of Sc+, Y+, and Lanthanide Ions with 1,3,5-tri-t-butylbenzene, W. W. Yin, A. G. Marshall, J. Marçalo, A. Pires de Matos, J. Am. Chem. Soc. 1994, 116, 8666-8672.
  • Laser Desorption Fourier Transform Mass Spectrometric Analysis of Organoactinides: Uranium and Thorium Polypyrazolylborates, Z. Liang, A. G. Marshall, J. Marçalo, N. Marques, A. Pires de Matos, I. Santos, D. A. Weil, Organometallics 1991, 10, 2794-2797.
  • A New Definition of Coordination Number and its Use in Lanthanide and Actinide Coordination and Organometallic Chemistry, J. Marçalo, A. Pires de Matos, Polyhedron 1989, 8, 2431-2437.
  • Actinide Poly(pyrazol-1-yl)borate Complexes: Synthesis and Structure of Hydrotris(3,5-dimethylpyrazol-1-yl)boratotrichloro-tetrahydrofuran Actinide (IV), M[HB(3,5-Me2pz)3]Cl3(THF) (M = Th and U), R. G. Ball, F. Edelmann, J. G. Matisons, J. Takats, N. Marques, J. Marçalo, A. Pires de Matos, K. W. Bagnall, Inorg. Chim. Acta 1987, 132, 137-143.
  • Evidence for Cathodic Electrodeposition of Radon Species, J. Marçalo, A. Pires de Matos, J. Radioanal. Nucl. Chem., Letters 1984, 86, 373-378.

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